Phase transitions and oxygen ordering in La2CoO4+δ and (T, T’)- La2CuO4: single crystal growth and structural studies using synchrotron and neutron diffraction methods
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Perovskite-type oxides of LaFe(1+x)O(3+δ) (x = 0.0, 0.2, 0.5 and 0.7) were synthesized by citrate sol–gel methodto ensure the formation of nanosized perovskites. The physicochemical properties of these LaFe(1+x)O(3+δ)materials were characterized by thermal gravimetric/differential analyses, Fourier transform infraredspectroscopy, X-ray powder diffraction, scanning electron and...
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Thl.: Ri elwc ld mc thod ofstructurl.: refinement from powder dilTr<:lction patterns is widely used with neutron data and int:reasingly so with x* ray data . [n this p<:lper the Ril.:tveld method has hccn cxplainl.:d. As an ex.ample the t: rystal :-.truclure of LazCu04 at rollm It:mperaturc has been refined using x*ray powder dirfr<:lctiol1 data. The crystal ,lruc lure is llflhorombi c wi...
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تاریخ انتشار 2011